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Synthesis, characterization and assessment thermal properties of clay based nanopigments

Mohammad Banimahd KIEVANI, Milad EDRAKI

《化学科学与工程前沿（英文）》 2015年 第9卷 第1期   页码 40-45 doi: 10.1007/s11705-015-1505-7

摘要： Nano-clay based pigments (NCP) are new type of pigments composed of organic dyes and layered silicate-clay nano-particles, and have already been used in polymeric coatings to improve mechanical thermal and stability properties. In this paper, the basic blue 41(BB41) was intercalated into Na - montmorillonite in an aqueous medium. The dye-intercalated montmorillonite was centrifuged, dried, and milled to prepare the nanopigment particles. X-ray diffraction showed an increase in the basal spacing, thus confirming intercalation of the BB41 molecules within the nanostructures of the interlayer spaces. Fourier transform infrared spectroscopy was used for identifying the functional groups and chemical bounding of Na -montmorillonite, BB41 and montmorillonite-BB41. The morphology of NCP was also studied by transmission electron microscopy. Finally, thermo-gravimetric analysis and differential thermograms suggested the thermal stability of the intercalated dye was improved.

关键词： nanopigment     layered silicate     cationic dye     thermal properties    

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Retraction note to: Synthesis, characterization and assessment thermal properties of clay based nanopigments

Mohammad Banimahd Kievani,Milad Edraki

《化学科学与工程前沿（英文）》 2016年 第10卷 第3期   页码 440-440 doi: 10.1007/s11705-016-1573-3

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An ANN-exhaustive-listing method for optimization of multiple building shapes and envelope propertieswith maximum thermal performance

Yaolin LIN, Wei YANG

《能源前沿（英文）》 2021年 第15卷 第2期   页码 550-563 doi: 10.1007/s11708-019-0607-1

摘要： With increasing awareness of sustainability, demands on optimized design of building shapes with a view to maximize its thermal performance have become stronger. Current research focuses more on building envelopes than shapes, and thermal comfort of building occupants has not been considered in maximizing thermal performance in building shape optimization. This paper attempts to develop an innovative ANN (artificial neural network)-exhaustive-listing method to optimize the building shapes and envelope physical properties in achieving maximum thermal performance as measured by both thermal load and comfort hour. After verified, the developed method is applied to four different building shapes in five different climate zones in China. It is found that the building shape needs to be treated separately to achieve sufficient accuracy of prediction of thermal performance and that the ANN is an accurate technique to develop models of discomfort hour with errors of less than 1.5%. It is also found that the optimal solutions favor the smallest window-to-external surface area with triple-layer low-E windows and insulation thickness of greater than 90 mm. The merit of the developed method is that it can rapidly reach the optimal solutions for most types of building shapes with more than two objective functions and large number of design variables.

关键词： ANN (artificial neural network)     exhaustive-listing     building shape     optimization     thermal load     thermal comfort    

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Thermal transport properties of monolayer phosphorene: a mini-review of theoretical studies

Guangzhao QIN, Ming HU

《能源前沿（英文）》 2018年 第12卷 第1期   页码 87-96 doi: 10.1007/s11708-018-0513-y

摘要： Phosphorene, a two-dimensional (2D) elemental semiconductor with a high carrier mobility and intrinsic direct band gap, possesses fascinating chemical and physical properties distinctively different from other 2D materials. Its rapidly growing applications in nano-/opto-electronics and thermoelectrics call for fundamental understanding of the thermal transport properties. Considering the fact that there have been so many studies on the thermal transport in phosphorene, it is on emerging demand to have a review on the progress of previous studies and give an outlook on future work. In this mini-review, the unique thermal transport properties of phosphorene induced by the hinge-like structure are examined. There exists a huge deviation in the reported thermal conductivity of phosphorene in literature. Besides, the mechanism underlying the deviation is discussed by reviewing the effect of different functionals and cutoff distance in calculating the thermal transport properties of phosphorene. It is found that the (vdW) interactions play a key role in the formation of resonant bonding, which leads to long-ranged interactions. Taking into account of the vdW interactions and including the long-ranged interactions caused by the resonant bonding with large cutoff distance are important for getting the accurate and converged thermal conductivity of phosphorene. Moreover, a fundamental insight into the thermal transport is provided based on the review of resonant bonding in phosphorene. This mini-review summarizes the progress of the thermal transport in phosphorene and gives an outlook on future horizons, which would benefit the design of phosphorene based nano-electronics.

关键词： thermal transport     phosphorene     resonant bonding    

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Thermal radiative properties of metamaterials and other nanostructured materials: A review

Ceji FU, Zhuomin M. ZHANG

《能源前沿（英文）》 2009年 第3卷 第1期   页码 11-26 doi: 10.1007/s11708-009-0009-x

摘要： The ability to manufacture, control, and manipulate structures at extremely small scales is the hallmark of modern technologies, including microelectronics, MEMS/NEMS, and nano-biotechnology. Along with the advancement of microfabrication technology, more and more investigations have been performed in recent years to understand the influence of microstructures on radiative properties. The key to the enhancement of performance is through the modification of the reflection and transmission properties of electromagnetic waves and thermal emission spectra using one-, two-, or three-dimensional micro/nanostructures. This review focuses on recent developments in metamaterials–manmade materials with exotic optical properties, and other nanostructured materials, such as gratings and photonic crystals, for application in radiative energy transfer and energy conversion systems.

关键词： metamaterial     nanostructured material     thermal radiative property     radiative energy transfer    

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of hierarchical nanohybrid CNT@Ni-PS and its applications in enhancing the tribological, curing and thermalproperties of epoxy nanocomposites

《化学科学与工程前沿（英文）》 2022年 第16卷 第10期   页码 1530-1530 doi: 10.1007/s11705-022-2240-5

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of hierarchical nanohybrid CNT@Ni-PS and its applications in enhancing the tribological, curing and thermalproperties of epoxy nanocomposites

Jinian Yang, Yuxuan Xu, Chang Su, Shibin Nie, Zhenyu Li

《化学科学与工程前沿（英文）》 2021年 第15卷 第5期   页码 1281-1295 doi: 10.1007/s11705-020-2007-9

摘要： Poor interfacial adhesion and dispersity severely obstruct the continued development of carbon nanotube (CNT)-reinforced epoxy (EP) for potential applications. Herein, hierarchical CNT nanohybrids using nickel phyllosilicate (Ni-PS) as surface decorations (CNT@Ni-PS) were synthesized, and the nanocomposites derived from varied mass fractions of EP and CNT@Ni-PS were prepared. The morphological structures, tribological performances, curing behaviors and thermal properties of EP/CNT@Ni-PS nanocomposites were carefully investigated. Results show that hierarchical CNT nanohybrids with homogeneous dispersion and well-bonded interfacial adhesion in the matrix are successfully obtained, presenting significantly improved thermal and tribological properties. Moreover, analysis on cure kinetics proves the excellent promotion of CNT@Ni-PS on the non-isothermal curing process, lowering the curing energy barrier steadily.

关键词： nickel phyllosilicate     surface decoration     tribological property     curing kinetics     thermal performance    

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Molecular dynamics investigation of mechanical properties of single-layer phagraphene

Ali Hossein Nezhad SHIRAZI

《结构与土木工程前沿（英文）》 2019年 第13卷 第2期   页码 495-503 doi: 10.1007/s11709-018-0492-4

摘要： Phagraphene is a very attractive two-dimensional (2D) full carbon allotrope with very interesting mechanical, electronic, optical, and thermal properties. The objective of this study is to investigate the mechanical properties of this new graphene like 2D material. In this work, mechanical properties of phagraphene have been studied not only in the defect-free form, but also with the critical defect of line cracks, using the classical molecular dynamics simulations. Our study shows that the pristine phagraphene in zigzag direction experience a ductile behavior under uniaxial tensile loading and the nanosheet in this direction are less sensitive to temperature changes as compared to the armchair direction. We studied different crack lengths to explore the influence of defects on the mechanical properties of phagraphene. We also investigated the temperature effect on the mechanical properties of pristine and defective phagraphene. Our classical atomistic simulation results confirm that larger cracks can reduce the strength of the phagraphene. Moreover, it was shown the temperature has a considerable weakening effect on the tensile strength of phagraphene. The results of this study may be useful for the design of nano-devices using the phagraphene.

关键词： phaqraphene     mechanical properties     crack propaqation     molecular dynamics     thermal effects    

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Experimental research on thermal transport properties of crystallized palladium-based alloys

Siyuan CHENG, Xuguo SHI, Weigang MA, Xing ZHANG, Guanglai LIU, Mingxiang PAN, Weihua WANG

《能源前沿（英文）》 2018年 第12卷 第1期   页码 121-126 doi: 10.1007/s11708-018-0531-9

摘要： Palladium-based alloy is a kind of material with a high glass forming ability and can be easily formed into an amorphous state. After an annealing process, it can also be maintained at a crystallized state. To study the thermal and electrical transport properties of crystallized palladium-based alloys, the steady-state T-type method, standard four-probe method, and AC heating-DC detecting T-type method were used to measure the thermal conductivity, electrical conductivity, and Seebeck coefficient of crystallized Pd Ni Cu P and Pd Ni Cu P alloys respectively. The results show that compared to amorphous samples, the thermal conductivity and electrical conductivity of crystallized palladium-based alloys are significantly higher, while the Seebeck coefficient is lower. The ratio of crystallized and amorphous thermal conductivity is higher for Pd Ni Cu P alloy fiber which has a higher glass forming ability, while the ratio of electronic thermal conductivity almost remains constant for both alloy fibers. The results also show that the slope of electrical resistivity to temperature is a function of elemental composition for crystallized quaternary palladium-based alloy fibers. The sensitivity of thermal conductivity and electrical conductivity to the composition is high, while the correlation between Seebeck coefficient and composition is relatively weak.

关键词： palladium-based alloy     T-type method     thermal conductivity     electrical conductivity     Seebeck coefficient    

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Studies on the rheological, phase morphologic, thermal and mechanical properties of poly(trimethylene

RUN Mingtao, SONG Hongzan, WANG Yingjin, YAO Chenguang, GAO Jungang

《化学科学与工程前沿（英文）》 2007年 第1卷 第3期   页码 238-245 doi: 10.1007/s11705-007-0043-3

摘要： The rheological, phase morphologic, thermal and mechanical properties of poly(trimethylene terephthalate)/metallocene polyethylene (PTT/mPE) blends in the presence of ethylene propylene diene monomer copolymer grafted with maleic anhydride (EPDM--MAH) as compatibilizer are studied by means of a capillary rheometer, scanning electron microscopy (SEM), differential scanning calorimetry (DSC) and thermogravimetric analyzer (TGA). Results suggest that the compatibility of PTT/mPE blends is improved greatly after the addition of a compatibilizer. The radius of the dispersed phase in the system decreases greatly when the compatibilizer is added into the blend. When the amount of compatibilizer exceeds 8 wt-%, the size of dispersed phase becomes larger again. This phenomena could be attributed to the higher viscosity of the EPDM--MAH phase, which is dispersed more difficulty in the PTT phase of lower viscosity, thus the mixing efficiency is apparently decreased during the melt blending process. Moreover, the melt viscosity of the blend reaches the maximal value in case of 4 wt-% compatibilizer content, above which it would decrease again. This result is associated with the generation of more and bigger dispersed phase inside the bulk phase, thus the grafting efficiency at the interface is decreased, which could result in lower viscosity. The DSC results suggest that the mPE component shows a nucleating effect, and could increase the overall degree and rate of PTT crystallization, while the addition of a compatibilizer might slightly diminish these effects. In addition, the blend with 4 wt-% compatibilizer shows the best thermal stability. Furthermore, the Izod impact strength and the tensile strength at room temperature of the blend are also markedly improved by the addition of a 4 8 wt-% compatibilizer.

关键词： /metallocene polyethylene     presence     rheological     phenomena     trimethylene terephthalate    

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典型硼化合物对毛竹热降解与燃烧性能的影响

杨守禄,吴义强,卿彦,姚春花

《中国工程科学》 2014年 第16卷 第4期   页码 51-55

摘要：

利用热重和锥形量热仪研究硼酸、硼砂两种典型硼化合物对毛竹热降解和燃烧性能的影响。结果 表明：硼酸、硼砂能降低竹材的最大热解速率，缩短高温热解区间，促进残炭生成。与未处理材相比，硼酸、硼砂明显减少竹材燃烧过程中的热量释放，热释放速率降至未处理材的50 %左右，总热释放量的降幅分别达50.6 %、44.1 %。硼酸、硼砂也能抑制竹材燃烧时的烟释放，总烟释放量分别下降95.3 %、91.6 %。硼酸、硼砂处理竹材能发挥高效的阻燃抑烟功效。

关键词： 硼酸     硼砂     毛竹     热降解     燃烧性能    

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mixed with three nominal maximum aggregate sizes in the bending beam rheometer on the prediction of thermalproperties of bituminous material

Chun-Hsing HO,María Francisca Martínez GONZÁLEZ,Cristina Pilar Martín LINARES

《结构与土木工程前沿（英文）》 2017年 第11卷 第1期   页码 1-7 doi: 10.1007/s11709-016-0367-5

摘要： The objective of this research is to evaluate an impact of asphalt mixture beams with varying sizes of aggregate in the Bending Beam Rheometer (BBR) for testing/predicting thermal cracking properties of asphalt pavements. The BBR test has following benefits: the equipment is cheaper, it uses smaller specimens, faster conditioning, easier availability for quality control, easier to manage, etc. However some concerns have been raised: some consider that the size of the aggregate may affect the test’s results; the other concern is that such small beams cannot represent the whole properties of the asphalt pavement. To address these criticisms, imaging techniques, statistical analysis, and viscoelastic modeling are used. Asphalt thin beams prepared with three different nominal maximum aggregate size (NMAS) (12.5mm, 9.5 mm, and 4.75 mm) were tested at three different temperatures (-18°C, -24°C, and -30°C). Based on results from statistical analyses and viscoelasticity, the ratio of asphalt binders and voids and stiffness differences among the three NMAS specimens are not significant, meaning that the impact of asphalt thin beams prepared with the three NMAS on the prediction of thermal cracking is minimal and can be neglected.

关键词： bending beam rheometer     thin beams     thermal cracking    

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Rosin side chain type catalyst-free vitrimers with high cross-link density, mechanical strength, and thermal

《化学科学与工程前沿（英文）》 2023年 第17卷 第9期   页码 1267-1279 doi: 10.1007/s11705-022-2291-7

摘要： The emergence of vitrimer, a new class of polymer materials can address the problem of recyclability, reprocess ability and recyclability of thermosetting plastics. Rosin, a natural product, is an ideal raw material for the preparation of polymers in a more sustainable way. Nevertheless, due to the huge steric hindrance caused by the hydrogenated phenanthrene ring structure, the cross-link density of materials is frequently lowered. In this study, hydrogenated rosin was adopted for preparing hydrogenated rosin side-chain type diacids, which were reacted with mixed epoxy to obtain rosin side-chain type vitrimers. It was completely characterized by differential scanning calorimetry test, thermogravimetric analysis, shape memory test and self-healing test. The prepared vitrimers exhibited good self-healing properties, excellent heat resistance (Td = 352 °C) as well as high mechanical properties (tensile strength of 46.75 MPa). The tricyclic diterpene structure of rosin was introduced into the side chain in order to avoid the reduction of cross-link density resulting from the huge steric hindrance of the rigid tricyclic hydrophenylene skeleton. Vitrimers can undergo dynamic transesterification reaction without external catalysts due to the autocatalytic effect of tertiary amines from epoxy. Moreover, our work expanded the application field of rosin, increased the added value of rosin, and provided a novel method for preparing rosin-based vitrimers with ideal properties.

关键词： vitrimers     rosin     catalyst-free     high mechanical properties     dynamic transesterification reaction    

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Effect of graphene and its derivatives on thermo-mechanical properties of phase change materials and

《能源前沿（英文）》 2022年 第16卷 第2期   页码 150-186 doi: 10.1007/s11708-021-0795-3

摘要： Phase change materials (PCMs) play a leading role in overcoming the growing need of advanced thermal management for the storage and release of thermal energy which is to be used for different solar applications. However, the effectiveness of PCMs is greatly affected by their poor thermal conductivity. Therefore, in the present review the progress made in deploying the graphene (Gr) in PCMs in the last decade for providing the solution to the aforementioned inadequacy is presented and discussed in detail. Gr and its derivatives ((Gr oxide (GO), Gr aerogel (GA) and Gr nanoplatelets (GNPs)) based PCMs can improve the thermal conductivity and shape stability, which may be attributed to the extra ordinary thermo-physical properties of Gr. Moreover, it is expected from this review that the advantages and disadvantages of using Gr nanoparticles provide a deep insight and help the researchers in finding out the exact basic properties and finally the applications of Gr can be enhanced.

关键词： phase change materials (PCMs)     graphene     thermal conductivity     characterization    

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Thermal cracking of waste printed wiring boards for mechanical recycling by using residual steam preprocessing

Yao CHEN, Jinhui LI, Huabo DUAN, Zhishi WANG

《环境科学与工程前沿（英文）》 2011年 第5卷 第2期   页码 167-174 doi: 10.1007/s11783-011-0308-4

摘要： Mechanical waste-processing methods, which combine crushing and separation processes for the recovery of valuable materials, have been widely applied in waste printed wiring board (PWB) treatment. However, both the high impact toughness and the tensile and flexural strengths of whole PWB with a laminated structure result in great energy consumption and severe abrasion of the cutters during multi-level crushing. In addition, the high temperatures occurring in continual crushing probably cause the decomposition of the polymer matrix. A thermal-crack method using residual steam as the heating medium has been developed to pre-treat waste PWBs. This treatment reduces the mechanical strength in order to improve the recovery rate of valuable materials in subsequent mechanical recycling. The changes of the PWBs’ macro-mechanical properties were studied to evaluate thermal expansion impacts associated with changes in temperature, and the dynamic dislocation micro-structures were observed to identify the fracture mechanism. The results showed that thermal cracking with steam at the temperature of 500 K can effectively attenuate the mechanical properties of waste PWBs, by reducing the impact, tensile and flexural strengths respectively, by 59.2%, 49.3% and 51.4%, compared to untreated PWB. Thermal expansion can also facilitate the separation of copper from glass fiber by reducing peel resistance by 95.4% at 500 K. It was revealed that the flexural fracture was a transverse cracking caused by concentrated stress when the heating temperature was less than 500 K, and shifted to a vertical cracking after exceeding 500 K.

关键词： waste printed wiring board (PWB)     residue steam     thermal-crack     mechanical properties    

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标题 作者 时间 类型 操作

Synthesis, characterization and assessment thermal properties of clay based nanopigments

Mohammad Banimahd KIEVANI, Milad EDRAKI

期刊论文

Retraction note to: Synthesis, characterization and assessment thermal properties of clay based nanopigments

Mohammad Banimahd Kievani,Milad Edraki

期刊论文

An ANN-exhaustive-listing method for optimization of multiple building shapes and envelope propertieswith maximum thermal performance

Yaolin LIN, Wei YANG

期刊论文

Thermal transport properties of monolayer phosphorene: a mini-review of theoretical studies

Guangzhao QIN, Ming HU

期刊论文

Thermal radiative properties of metamaterials and other nanostructured materials: A review

Ceji FU, Zhuomin M. ZHANG

期刊论文

of hierarchical nanohybrid CNT@Ni-PS and its applications in enhancing the tribological, curing and thermalproperties of epoxy nanocomposites

期刊论文

of hierarchical nanohybrid CNT@Ni-PS and its applications in enhancing the tribological, curing and thermalproperties of epoxy nanocomposites

Jinian Yang, Yuxuan Xu, Chang Su, Shibin Nie, Zhenyu Li

期刊论文

Molecular dynamics investigation of mechanical properties of single-layer phagraphene

Ali Hossein Nezhad SHIRAZI

期刊论文

Experimental research on thermal transport properties of crystallized palladium-based alloys

Siyuan CHENG, Xuguo SHI, Weigang MA, Xing ZHANG, Guanglai LIU, Mingxiang PAN, Weihua WANG

期刊论文

Studies on the rheological, phase morphologic, thermal and mechanical properties of poly(trimethylene

RUN Mingtao, SONG Hongzan, WANG Yingjin, YAO Chenguang, GAO Jungang

期刊论文

典型硼化合物对毛竹热降解与燃烧性能的影响

杨守禄,吴义强,卿彦,姚春花

期刊论文

mixed with three nominal maximum aggregate sizes in the bending beam rheometer on the prediction of thermalproperties of bituminous material

Chun-Hsing HO,María Francisca Martínez GONZÁLEZ,Cristina Pilar Martín LINARES

期刊论文

Rosin side chain type catalyst-free vitrimers with high cross-link density, mechanical strength, and thermal

期刊论文

Effect of graphene and its derivatives on thermo-mechanical properties of phase change materials and

期刊论文

Thermal cracking of waste printed wiring boards for mechanical recycling by using residual steam preprocessing

Yao CHEN, Jinhui LI, Huabo DUAN, Zhishi WANG

期刊论文